Identification of characteristic flavor markers in breakable capsules for flavoring by GC/MS combined with multivariate statistical analysis

Authors

ZHANG Hua, Technology Center, China Tobacco Jiangsu Industrial Co., Ltd., Nanjing, Jiangsu 210019, China
LIU Qi, Technology Center, China Tobacco Jiangsu Industrial Co., Ltd., Nanjing, Jiangsu 210019, China
YE Yuan-qing, Technology Center, China Tobacco Jiangsu Industrial Co., Ltd., Nanjing, Jiangsu 210019, China
ZHU Huai-yuan, Technology Center, China Tobacco Jiangsu Industrial Co., Ltd., Nanjing, Jiangsu 210019, China
LIAO Hui-yun, Technology Center, China Tobacco Jiangsu Industrial Co., Ltd., Nanjing, Jiangsu 210019, China

Abstract

Objective: Identify the characteristic markers for the quality control of breakable capsule flavor. Methods: Volatile and semi-volatile compounds were detected by GC/MS, and the fingerprinting of the target samples was established. The obtained data were analyzed by multivariate statistical analysis. Results: 27 kinds of volatile and semi-volatile substances were identified, including 20 dominant aroma compounds and 7 shell materials, which were limonene, eugenol, anethole, menthol and so on, and caprylic/capric triglyceride respectively. Under the optimized conditions, the instrument precision, intra-day precision and inter-day precision were between 0.56%～9.94%, 3.07%～9.81% and 2.81%～11.95% respectively. Combined with the nearest neighbor algorithm of ChemPattern software, GC/MS fingerprinting of the sample was established. PCA showed there were no significant difference between the normal and simulated breakable capsule flavor samples. However, based on the results of OPLS-DA, four compounds were identified as characteristic markers （variable importance projection value>1, P<0.05）, which were limonene, methyl octanoate, methyl decanoate and eugenol, respectively. In general, these characteristic substances can reflect the fragrant type of breakable capsule flavor. Conclusion: This study can provide a reference for the quality control of breakable capsule flavor.

Publication Date

9-28-2021

First Page

37

Last Page

43,65

DOI

10.13652/j.issn.1003-5788.2021.09.006

Recommended Citation

Hua, ZHANG; Qi, LIU; Yuan-qing, YE; Huai-yuan, ZHU; and Hui-yun, LIAO (2021) "Identification of characteristic flavor markers in breakable capsules for flavoring by GC/MS combined with multivariate statistical analysis," Food and Machinery: Vol. 37: Iss. 9, Article 6.
DOI: 10.13652/j.issn.1003-5788.2021.09.006
Available at: https://www.ifoodmm.cn/journal/vol37/iss9/6

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