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Corresponding Author(s)

李勇(1987—),男,江苏省农业科学院副研究员,博士。E-mail: liyong201508@jaas.ac.cn余向阳(1972—),男,江苏省农业科学院研究员,博士。E-mail: yuxy@jaas.ac.cn

Abstract

Objective: This study aimed to investigate the residues and risk assessment of pesticides in peach gum. Methods: The quantitative analysis of 44 pesticide residues in peach gum was established based on liquid chromatography tandem-mass spectrometry (LC-MS/MS), and the pesticide residues in 173 peach gum samples were detected as well as the risk assessment of pesticide residues. Results: The limits of detection (LOD) and the limits of quantification (LOQ) of 44 kinds of pesticides in this quantitative method were between 0.05~1.80 μg/kg and 0.20~2.42 μg/kg, respectively. Recoveries of these pesticides ranged from 61.77%~119.48%. In 173 peach gum samples, 22 out of 44 pesticides were detected and the total detection rate of pesticides in peach gum was 98.8%. The detection rate of difenoconazole was the highest (95%), followed by chlorpyrifos (54%), carbendazim (34%), furamethoxam (32%) and pyraclostrobin (19%). The average residue of difenoconazole in different peach gum samples was the highest (0.332 mg/kg), followed by furamethoxam (0.093 mg/kg), carbendazim (0.061 mg/kg) and chlorpyrifos (0.033 mg/kg). Conclusion: Pesticide residues in peach gum were related to the usage of pesticides in peach production and were at a low risk level. It is recommended to pick peach gum from August to October.

Publication Date

6-9-2023

First Page

55

Last Page

63,100

DOI

10.13652/j.spjx.1003.5788.2022.80705

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