Abstract
[Objective] To enhance the quality and market value of original bottled Maotai -flavored Baijiu, this study investigates the effects of microwave irradiation on major flavor compounds during the aging process and optimizes the microwave -assisted aging process. [Methods] Maotai -flavored Baijiu samples were subjected to microwave irradiation, and the effects of irradiation time, irradiation temperature, and power density on the contents of key flavor compounds, including ethyl acetate, ethyl lactate, ethyl butyrate, ethyl hexanoate, acetic acid, and acetaldehyde, were examined in samples stored for 28 days after treatment. [Results] With increasing irradiation time, ester contents first increased and then fluctuated and decreased, while acetic acid and acetaldehyde contents first increased, then decreased, and increased again. As the irradiation temperature increased, ester and acetic acid contents first increased, then slightly |decreased, and finally reached a new peak, whereas acetaldehyde content first increased and then fluctuated and decreased. With increasing power density, the contents of esters, acetic acid, and acetaldehyde all first increased and then decreased. According to the results, under the optimal microwave conditions of 45 min irradiation time, 50 ℃ irradiation temperature, and 1.0 W/mL power density, ethyl acetate, ethyl lactate, ethyl butyrate, ethyl hexanoate, and acetic acid increased by 10.1%, 10.0%, 8.6%, 7.9%, and 9.7%, respectively, compared with untreated samples. [Conclusion] Under the optimized process parameters, microwave irradiation promotes the formation of esters and acids, thereby accelerating the aging process of Maotai -flavored Baijiu.
Publication Date
10-21-2026
First Page
214
Last Page
219
DOI
10.13652/j.spjx.1003.5788.2025.80322
Recommended Citation
Jimin, Huang; Haibo, Qin; Zhaolong, Wu; Guohui, Zhao; Jinzhi, Liang; Bingzheng, Li; and Zhimin, Huang
(2026)
"Effects of microwave irradiation on major flavor compounds in Maotai-flavor Baijiu with original bottled packaging,"
Food and Machinery: Vol. 42:
Iss.
9, Article 24.
DOI: 10.13652/j.spjx.1003.5788.2025.80322
Available at:
https://www.ifoodmm.cn/journal/vol42/iss9/24
References
[1] GB/T 15109—2021 白酒工业术语 [S].GB/T 15109—2021 Terminology of Baijiu industry [S].
[2] Wang G N,Song X B,Zhu L,et al.A flavoromics strategy for the differentiation of different types of Baijiu according to the non-volatile organic acids [J].Food Chemistry,2022,374:131641.
[3] 秦丹,段佳文,李有明,等.白酒老熟过程中风味成分的变化及人工催陈技术的研究进展 [J].食品科学,2021,42(23):260-267.Qin D,Duan J W,Li Y M,et al.A review of changes of flavor compounds during Baijiu aging and recent progress in artificial aging techniques [J].Food Science,2021,42(23):260-267.
[4] 邱重晏,王万能,王东,等.清香型白酒快速陈酿化的初步研究[J].酿酒,2011,38(6):26-29.Qiu C Y,Wang W N,Wang D,et al.Preliminary study on accelerated aging Fen-flavor Liquor [J].Liquor Making,2011,38(6):26-29.
[5] He J,Chen Q,Jia X,et al.The effects of gamma irradiation and natural aging on the composition of Nongxiangxing Baijiu [J].Journal of Food Processing and Preservation,2022,46(12):e17146.
[6] Zhu S M,Xu M L,Ramaswamy H S,et al.Effect of high pressure treatment on the aging characteristics of Chinese liquor as evaluated by electronic nose and chemical analysis [J].Scientific Reports,2016,6:30273.
[7] Zhang W,Xiao Y,Deng R J,et al.An electric-field instrument for accelerated aging to improve flavor of Chinese Baijiu [J].LWT-Food Science & Technology,2023,174:114446.
[8] 魏群舒,杨勇,陈雨,等.超声波催陈米香型白酒的研究 [J].中国酿造,2017,36(10):66-70.Wei Q S,Yang Y,Chen Y,et al.Accelerating aging of rice-flavor Baijiu by ultrasonic wave [J].China Brewing,2017,36(10):66-70.
[9] 王本盛,张莉丽,赵瑞,等.高能电子束辐照酱香型白酒的催陈效应 [J].食品科技,2021,46(9):79-86.Wang B S,Zhang L L,Zhao R,et al.Aging effect of Maotai-flavor liquor irradiated by high energy electron beam [J].Food Science and Technology,2021,46(9):79-86.
[10] 张大力,冯艳鹤,修琳,等.超高压技术对白酒催陈作用的影响[J].食品工业,2018,39(7):23-28.Zhang D L,Feng Y H,Xiu L,et al.Effect of ultra-high pressure technology on the aging of liquor [J].The Food Industry,2018,39(7):23-28.
[11] Liu Y,He F,Shi Y,et al.Effect of the high pressure treatments on the physicochemical properties of the young red wines supplemented with pyruvic acid [J].Innovative Food Science & Emerging Technologies,2018,48:56-65.
[12] Jia W,Fan Z B,Du A,et al.Untargeted foodomics reveals molecular mechanism of magnetic field effect on Feng-flavor Baijiu ageing [J].Food Research International,2021,149:110681.
[13] Dai N,Zhang X,Cai Z P,et al.The effect of different pulsed magnetic field and microwave composite treatment on the aroma compounds and sensory characteristics of soy-sauce flavor Chinese liquor [J].CyTA - Journal of Food,2021,19(1):793-804.
[14] Xiong A Y,Zhao K,Hu Y R,et al.Influence of electrochemical oxidation on the maturation process of the distilled spirit [J].ACS Omega,2020,5(29):18 349-18 355.
[15] 蒋祥瑞,蒋燕明,张娟,等.白酒人工催陈技术研究进展 [J].食品工业科技,2021,42(17):389-396.Jiang X R,Jiang Y M,Zhang J,et al.Research advances in artificial aging technology of Baijiu [J].Science and Technology of Food Industry,2021,42(17):389-396.
[16] 吴知非,梁慧珍,刘正,等.白酒陈酿机理及催陈技术研究现状[J].食品研究与开发,2022,43(13):196-202.Wu Z F,Liang H Z,Liu Z,et al.Research status of liquor aging mechanisms and technology [J].Food Research and Development,2022,43(13):196-202.
[17] 杨婷,农绍庄,刘畅,等.白酒的微波陈化研究 [J].食品工业,2014,35(2):109-112.Yang T,Nong S Z,Liu C,et al.Study on aging of liquor by microwave [J].The Food Industry,2014,35(2):109-112.
[18] 江倩,刘建学,李佩艳,等.微波辐射处理对浓香型白酒中挥发性物质的影响 [J].核农学报,2022,36(2):341-349.Jiang Q,Liu J X,Li P Y,et al.Effect of microwave radiation treatment on volatile substances in Luzhou-flavor liquor [J].Journal of Nuclear Agricultural Sciences,2022,36(2):341-349.
[19] 代佳慧,刘建学,韩四海,等.微波辐射对浓香型白酒中乙酸和乙酸乙酯的影响 [J].食品与机械,2019,35(2):33-36,54.Dai J H,Liu J X,Han S H,et al.Effect of microwave radiation on acetic acid and ethyl acetate in Luzhou-flavor liquor [J].Food & Machinery,2019,35(2):33-36,54.
[20] 江倩,刘建学,李佩艳,等.微波辐射处理对浓香型白酒中甲醇和乙醛的影响 [J].微波学报,2021,37(3):92-98.Jiang Q,Liu J X,Li P Y,et al.Effect of microwave radiation treatment on methanol and acetaldehyde in Luzhou-flavor liquor [J].Journal of Microwaves,2021,37(3):92-98.
[21] Jia W,Li Y L,Du A,et al.Foodomics analysis of natural aging and gamma irradiation maturation in Chinese distilled Baijiu by UPLC-Orbitrap-MS/MS [J].Food Chemistry,2020,315:126308.
[22] 申圣丹,王盛民,刘睿颖.超高压射流技术对白酒的催陈作用[J].食品科技,2012,37(4):83-85.Shen S D,Wang S M,Liu R Y.Effectiveness of ultra-high incoming on liquor aging [J].Food Science and Technology,2012,37(4):83-85.
[23] Zhu L,Song X B,Li X,et al.Interactions between kafirin and pickle-like odorants in soy sauce flavor Baijiu:aroma profile change and binding mechanism [J].Food Chemistry,2023,400:133854.
[24] 张满满,谢康俊,齐伟,等.电子束辐照陈化大曲白酒和小曲白酒 [J].辐射研究与辐射工艺学报,2018,36(5):39-45.Zhang M M,Xie K J,Qi W,et al.Electron-beam irradiation aging of Daqu liquor and Xiaoqu liquor [J].Journal of Radiation Research and Radiation Processing,2018,36(5):39-45.
[25] Hong J X,Huang H,Zhao D R,et al.Investigation on the key factors associated with flavor quality in northern strong aroma type of Baijiu by flavor matrix [J].Food Chemistry,2023,426:136576.
