Encapsulation in glassy carbohydrates via extrusion is the low temperature technology and considered to be suitable for encapsulating heat-sensitive materials. The selection of matrix is the important factor. The temperatures of extruder barrel were T1 (65 ℃),T2 (85 ℃),T3 (105 ℃) and T4 (95 ℃). Screw speed was 60 r/min and the feeding speed was 1.2 kg/h. The effects of matrix including maltodextrin, maltodextrin added sucrose and maltodextrin added modified starch on the extrudates was investigated. The results showed that the extruded products were the glassy state. The glass transition temperature (Tg) of the extrudate used maltodextrin as only matrix were 48.52 ℃. Adding sucrose to maltodextrin made Tg of extrudate decrease. While adding modified starch to maltodextin made Tg of extrudate increase. With the temperature increasing, the glassy state was destroyed and orange oil released gradually from thermogravimetric analysis. The release rate of orange oil was slower from composite matrix than single matrix. The results of scanning electron micrographs showed that orange oil was dispersed with small oil drops in glassy carbobydrates.

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[1] 鲁丁丁. 甜橙油纳米乳的构建及其稳定性研究[D]. 杭州: 浙江工商大学, 2014.
[2] Reineccius G. Flavor chemistry and technology[M]. 2nd. Boca Raton: Taylor & Francis Routledge, 2006.
[3] 吴克刚, 孔令会, 武伟. 玻璃化微胶囊香精的研究[J]. 食品科学, 2003, 24(11):84~88.
[4] 蔡茜彤, 段小明, 冯叙桥, 等. 微胶囊技术及其在食品添加剂中的应用与展望[J]. 食品与机械, 2014, 30(4): 247~251.
[5] Tackenberg M W, Krauss R, Marmann A, et al. Encapsulation of liquids using a counter twin screw extruder[J]. European Journal of Pharmaceutics and Biopharmaceutics, 2015(89): 9~17.
[6] Emin M A, Schuchmann H P. Analysis of the dispersive efficiency in a twin-screw extrusion processing of starch based matrix[J]. Journal of Food Engineering, 2013(115): 132~143.
[7] 武伟, 杨连生. 玻璃化香精[J]. 香料香精化妆品, 2002(2): 28~30.
[8] Dawei C, Shabbar A, Khizar H, et al. Encapsulation of ascorbic acid in amorphous maltodextrin employing extrusion as affected by matrix/core ratio and water content [J]. International Journal
[9] 常大伟, 张晓鸣, 夏书芹, 等. 低聚异麦芽糖为基质挤压法制备玻璃化抗坏血酸胶囊[J]. 食品与生物技术学报, 2011, 30(2): 185~189.
[10] 梁蓉. 以OSA变性淀粉为乳化剂的纳米乳液制备及特征研究[D]. 无锡: 江南大学, 2013.
[11] Tackenberg M W, Thommes M, Schuchmann H P, et al. Solid state of processed carbohydrate matrices from maltodextrin and sucrose [J]. Journal of Food Engineering, 2014(129): 30~37.
[12] Carolina B C, Carolina S, Zamora M, et al. Glass transition temperature and some physical and sensory changes in stored spray-dried encapsulated flavors [J]. LWT-Food Science and Technology, 2007(40): 1 792~1 797.
[13] Buera P, Schebor C, Elizalde B. Effects of carbohydrate crystallization on stability of dehydrated foods and ingredient formulations [J]. Journal of Food Engineering, 2005(67): 157~165.
[14] 何健. 论食品的玻璃化保藏[J]. 郑州轻工业学院学报(自然科学版), 2002, 17(3): 54~57.
[15] 林向阳, 阮榕生, 何承云, 等. 快速测量食品玻璃化转变温度新方法的研究[J]. 食品科学, 2005, 26(3): 269~271.
[16] Bhandari B R, Howes T. Implication of glass transition for the drying and stability of dried foods[J]. Journal of Food Engineering, 1999(40): 71~79.
[17] Champion D, Le Meste M, Simato D. Towards an improved understanding of glass transition and relaxations in foods-molecular mobility in the glass transition range[J]. Trends in Food Science Technology, 2000(11): 41~55.
[18] 吴克刚, 钱银川. 玻璃化微胶囊化技术[J]. 食品科学, 2002, 23(8): 324~327.
[19] Pothakamury U R, Barbosa-Cánovas G V. Fundamental aspects of controlled release in foods [J]. Trends in Food Science & Technology, 1995(6): 397~406.

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