Analysis of components of oleoresin of cold drawn oil in Zanthoxylum with different extraction methods
To discuss the effects with different methods of oleoresin of cold pressing oil in Zanthoxylum extraction, select appropriate oleoresin extraction method, and explore different extraction methods of oleoresin flavor components of cold pressing oil in Zanthoxylum. With the cold pressing oil in Zanthoxylum as raw material, water bath, ultrasonic and microwave methods were used to extract the oleoresin and GC—MS was adopted to analyze flavor components of the different extraction methods of oleoresin. The results showed that the extraction of oleoresin absorbance at 270 nm value of ultrasound is the highest, followed by water bath, the lowest is microwave; the optimum conditions of ultrasonic extraction were obtained by orthogonal test, that is ratio of material to liquid 1∶20(m∶V), power 400 W, temperature 40 ℃, time 40 min. GC—MS analysis results indicated that oleoresin obtained by organic solvent extraction contains rich flavor components, but the kinds and contents of oleoresin extracted by different methods were different. The constituents of oleores which was extracted by ultrasonic was the maximum, and the relative contents of main flavor substances were the highest (linalool was as high as 63.07%, limonene was 4.62%, methyl linoleate was 5.11% ). The water bath were second, microwave extraction were the lowest. The results lay a foundation for the development and utilization of oleoresin of Zanthoxylum.
Yan, JIANG; Biao, PU; Hanqing, WANG; Lin, XU; Yachao, FENG; and Yan, CHEN
"Analysis of components of oleoresin of cold drawn oil in Zanthoxylum with different extraction methods,"
Food and Machinery: Vol. 32:
1, Article 32.
Available at: https://www.ifoodmm.cn/journal/vol32/iss1/32
［1］ 张华. 青花椒的结实特性及营养成分的研究［D］. 雅安: 四川农业大学, 2011: 2-4.
［2］ 付苗苗. 花椒中麻味物质的提取分离及纯化工艺的研究［D］. 西安: 西北大学, 2010: 1-10.
［3］ 李宏梁, 薛婷. 花椒果皮的研究进展［J］. 中国调味品, 2014, 39(1): 124-128.
［4］ 张怀予, 王军节, 陈园凡, 等. 水蒸气蒸馏法提取花椒精油及挥发性成分分析［J］. 食品与发酵工业, 2014, 40(7): 166-171.
［5］ 赵志峰. 汉源花椒风味物质研究及花椒油生产工艺优化［D］. 成都: 四川大学, 2005: 9-12.
［6］ 张郁松. 花椒风味物质超临界萃取与有机溶剂萃取的比较［J］. 中国调味品, 2014, 39(2): 25-27.
［7］ 祝瑞雪, 曾维才, 赵志峰, 等. 汉源花椒精油的化学成分分析及其抑菌作用［J］. 食品科学, 2011, 32(17): 85-88.
［8］ 莫彬彬, 连宾, 万固存, 等. 超临界CO2分步萃取花椒香气和麻味物质的初步研究［J］. 食品科学, 2009, 30(8): 201-203.
［9］ 杜双奎, 于修烛, 王青林, 等. 超声波辅助提取亚麻籽油的研究［J］. 中国粮油学报, 2009, 24(4): 70-73.
［10］ 杜若源, 谢晶, 王婷, 等. 超声波辅助提取银杏叶中总黄酮的工艺优化［J］. 食品与机械, 2015, 31(1): 167-170.
［11］ Zhao Bing, Yin Hui. Technology of the ultrasonic-circulated extraction and its application in the research and manufactory of herbal drugs［J］. Chinese Traditional and Herbal Drugs, 2006, 37(1): 154-156.
［12］ Pan Ying-ming, Wang Kai, Huang Si-qin, et al. Antioxidant activity of microwave-assisted extract of Longan (Dimocarpus Longan Lour.) peel［J］. Food Chemistry, 2008, 106(3): 1 264-1 270.
［13］ 王正宽, 周茆, 刘圆, 等. 微波技术在桂枝茯苓胶囊提取过程中的应用［J］. 中国中药杂志, 2015, 40(11): 2 123-2 127.
［14］ 姜欢笑, 蒲彪, 周婷, 等. 超声波辅助提取花椒冷榨油饼粕中油脂的工艺优化［J］. 食品工业科技, 2014, 35(21): 220-223.
［15］ 李东, 左勇, 邹杰, 等. 藤椒油微波提取工艺研究［J］. 中国调味品, 2013, 38(9): 85-88.