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Abstract

To make full use of Idesia polycarpa resource, the optimum conditions of extracting oil in I. Polycarpa by supercritical CO2 were studied by single factor and Box- Behnken designs, and the fatty acid composition of this oil was analyzed by gas chromatography-mass spectrometry (GC-MS). The results showed that the yield of the oil in I. polycarpa extracted by supercritical CO2 was (38.25±0.41)%, when extracted at 24 MPa and 53 ℃ for 147 min. Moreover, the regression model between yield and influence factors was very significant (P=0.000 9). In addition, the results of GC-MS showed that the total content of unsaturated fatty acid in the oil was 81.33%, and that of linoleic acid was 71.43%. In conclusion, the oil extracted from I. polycarpa is an edible oil resource with high quality, and could be efficiently extracted by using supercritical CO2.

Publication Date

11-28-2016

First Page

154

Last Page

157,228

DOI

10.13652/j.issn.1003-5788.2016.11.035

References

[1] 吴全珍. 我国毛叶山桐子开发利用回顾和展望[J]. 中国油脂, 2011, 36(6): 54-57.
[2] 龚榜初, 李大伟, 江锡兵, 等. 不同产地山桐子果实含油率及其理化指标变异分析[J]. 西北植物学报, 2012, 32(8): 1 680-1 685.
[3] 郭华, 沈泉维, 胡尧超. 山桐子油的品质分析[J]. 现代食品科技, 2012, 28(3): 345-347, 363.
[4] YANG Fang-xia, SU Yin-quan, LI Xiu-hong, et al. Preparation of biodiesel from Idesia polycarpavar. vestita fruit oil[J]. Industrial crops and products, 2009, 29(2/3): 622-628.
[5] 朱卫霞, 杜开峰, 汪全义, 等. 毛叶山桐子油制备环境友好型润滑油的研究[J]. 粮油加工, 2010(12): 56-60.
[6] 陈姹月, 唐琳, 陈放. 7种木本植物油理化性质及其生物柴油脂肪酸组成的比较研究[J]. 西南师范大学学报: 自然科学版, 2012, 37(12): 88-92.
[7] 刘春雷, 江连洲,于殿宇, 等. 山桐子油提取工艺的研究及脂肪酸组成分析[J]. 食品科技, 2012, 37(2): 192-196.
[8] 龚榜初, 李大伟, 江锡兵, 等. 不同种源山桐子果实脂肪酸组成变异分析[J]. 植物生理学报, 2012, 48(5): 505-510.
[9] KRIS-ETHERTON P M, HARRIS W S, APPEL L J, et al. Fish consumption, fish oil, omega-3 fatty acids, and cardiovascular disease[J]. Circulation, 2002, 106(21): 2 747-2 757.
[10] NESTEL P, CLIFTON P, COLQUHOUN D, et al. Indications for omega-3 long chain polyunsaturated fatty acid in the prevention and treatment of cardiovascular disease[J]. Heart, Lung and Circulation, 2015, 24(8): 769-779.
[11] SIRI-TARINO P W, CHIU S, BERGERON N, et al. Saturated fats versus polyunsaturated fats versus carbohydrates for cardiovascular disease prevention and treatment[J]. Annual Review of Nutrition, 2015, 35: 517-543.
[12] 吴发旺, 刘春雷. 响应面优化冷榨法制取山桐子油工艺的研究[J]. 食品工业科技, 2012, 33(11): 278-282.
[13] 华婉, 叶扬, 王战国, 等. 山桐子油的提取分离及理化性质研究[J]. 四川大学学报: 自然科学版, 2016, 53(1): 181-186.
[14] 杨朝福, 霍阿丽, 陆刚, 等. 均匀设计优化水冬瓜果实油脂的提取工艺[J]. 中国粮油学报, 2009, 24(3): 75-78.
[15] 周海旭, 李忠海, 张慧, 等. 微波辅助提取樟树叶木脂素工艺优化[J]. 食品与机械, 2016, 32(6): 193-197.
[16] 滕国生, 刘勇, 武丽达, 等. 响应面优化L-赖氨酸培养基[J]. 食品与机械, 2016, 31(5): 256-260.
[17] 中国国家技术监督局. GB/T 17376—2008 动植物油脂脂肪酸甲酯制备[S]. 北京: 中国标准出版社, 2009.
[18] 中国国家技术监督局. GB/T 17377—2008 动植物油脂脂肪酸甲酯的气相色谱分析[S]. 北京: 中国标准出版社, 2009.
[19] 赖锡湖, 黄卓, 李坚, 等. 超临界CO2萃取茶叶籽油及其成分分析[J]. 食品与机械, 2011, 27(2): 38-40.
[20] 汤鹏, 段海霞, 夏金梅, 等.响应面法优化超临界CO2萃取鲍鱼内脏油脂及其脂肪酸种类测定[J]. 食品科学, 2015, 36(12): 153-159.
[21] 贺绍琴, 张君萍, 阿布力米提·伊力, 等. 莴苣籽油的超临界CO2萃取工艺及其脂肪酸组成分析[J]. 中国油脂, 2015, 40(1): 1-5.
[22] 王亚琦, 陈奕洪, 黄卫文, 等. 超临界CO2萃取崖柏精油的研究[J]. 食品与机械, 2015, 31(3): 175-178.
[23] 刘光敏, 徐响, 高彦祥. 超临界CO2萃取草莓籽油工艺研究及其对脂肪酸组成的影响[J]. 中国粮油学报, 2009, 24(3): 84-88.
[24] DA PORTO C, DECORTI D, TUBARO F. Fatty acid composition and oxidation stability of hemp (Cannabis sativa L.) seed oil extracted by supercritical carbon dioxide [J]. Industrial Crops and Products, 2012, 36(1): 401-404.
[25] 程丹, 傅玉颖, 梅子, 等. 响应曲面法优化酵母微胶囊化核桃油工艺[J]. 中国食品学报, 2013, 13(11): 28-34.

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