Abstract
The hollow fiber liquid phase microextraction high performance liquid chromatography (HF—LPME—HPLC) of bisphenol A in canned food were determined to establish a simple, fast and accurate detection method. Mainly use the two-phase hollow fiber (HF) of liquid phase microextraction (LPME) technology, combined with high performance liquid chromatography to the determination of bisphenol A (BPA) content, so as to realize the optimization of the extractant, sample solution pH, extraction temperature, extraction time and stirring rate and other basic data parameters optimization,The results of the study show that: to octanol as the extractant, the selection of the determination of food sample solution pH value of 6.1, and the corresponding extraction temperature is 40 degrees Celsius for 40 min, relative standard deviation was 4.3%. The detection limit was 12.7 g/L and bisphenol A in food sample enrichment times the number reached 200 times, the average sample recovery rate in between 86.1%～105%.
Publication Date
3-28-2016
First Page
93
Last Page
95,121
DOI
10.13652/j.issn.1003-5788.2016.03.019
Recommended Citation
Huanhuan, DAI
(2016)
"Determination of bisphenol A in canned food by HPLC method,"
Food and Machinery: Vol. 32:
Iss.
3, Article 19.
DOI: 10.13652/j.issn.1003-5788.2016.03.019
Available at:
https://www.ifoodmm.cn/journal/vol32/iss3/19
References
[1] 张彦丽, 任佳丽, 李忠海, 等. 食品包装材料中双酚A的研究进展[J]. 食品与机械, 2011, 27(1): 155-157.
[2] 夏英, 张澜, 赵尔成, 等. 分散固相萃取/分散液液微萃取—气相色谱法测定甘蓝中的拟除虫菊酯类农药残留[J]. 分析测试学报, 2014, 33(2): 192-196.
[3] 高明慧, 周仕林, 杨卓圆, 等. 氨基酸—乙酰丙酮分光光度法测定水样中甲醛[J]. 理化检验: 化学分册, 2014, 50(1): 50-53.
[4] 赵海香, 刘海萍, 闫早婴. 多壁碳纳米管固相萃取净化—高效液相色谱法测定猪肉和鸡肉中的磺胺多残留[J]. 色谱, 2014(3): 294-298.
[5] 方晓明, 周浩, 冯春野, 等. 高效液相色谱/荧光法测定罐头食品中双酚A类物质的研究[J]. 分析测试学报, 2014, 33(12): 1 393-1 398.
[6] 吴茵琪, 钟月香, 蒋小良, 等. 微波萃取－高效液相色谱法测定食品塑料包装材料中双酚A含量[J]. 包装与食品机械, 2015(3): 62-65.
[7] 黄艳红, 丁健桦, 邱昌福, 等. 液相微萃取高效液相色谱法测定乳制品中的三聚氰胺[J]. 食品科学, 2010, 31（2）： 161-164.