Abstract
Based on GB 23200.92-2016, the samples were detected, and a mathematical model was established. Moreover, each uncertainty of the whole analysis procedures was analyzed and quantified. It was found that, when the pentachlorophenol residue was 14 μg/kg, the extended uncertainty was 3 μg/kg (k=2) under the 95% confidence interval. The results showed that the main sources of measurement uncertainties are derived from the final volume of sample, measurement repeatability, standard solution preparation, and the calibration fitting.
Publication Date
9-28-2019
First Page
84
Last Page
88
DOI
10.13652/j.issn.1003-5788.2019.09.016
Recommended Citation
Li, OUYANG; Hui, WANG; Yi, HE; Yaya, CHEN; Tingshu, HU; and Manshu, LIU
(2019)
"Evaluation of uncertainty for the determination of pentachlorophenol in pork liver by ultra-high performance liquid chromatography-tandem mass spectrometry,"
Food and Machinery: Vol. 35:
Iss.
9, Article 16.
DOI: 10.13652/j.issn.1003-5788.2019.09.016
Available at:
https://www.ifoodmm.cn/journal/vol35/iss9/16
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