•  
  •  
 

Abstract

The samples of Anyue ceramic-pot sealed meat produced in January, April, July and October were collected and analyzed by electronic nose, electronic tongue and headspace solid phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS). Artificial sensory evaluation showed that there was no significant difference in the flavor of each Anyue ceramic-pot sealed meat sample (P>0.05). Electronic nose analysis showed that Anyue ceramic-pot sealed meat had significant difference in odor between January and April (P<0.05), while other samples had no significant difference (P>0.05). Electronic tongue analysis showed that Anyue ceramic-pot sealed meat produced in January and October had significant difference in taste (P<0.01), and other samples also had significant difference (P<0.05). GC-MS analysis showed that there were significant differences in the types and relative contents of volatile substances among the samples. 53 kinds of volatile substances were detected in the ceramic-pot sealed meat of January, and 56 kinds of them were detected in the ceramic-pot sealed meat of April, with the relative content of volatile substances as high as 88.60%. 73 kinds of volatile substances were detected in the ceramic-pot sealed meat of July, with the relative content of volatile substances only 50.68%, and 70 kinds of them were detected in the ceramic-pot sealed meat of October. The characteristic flavor substances in fermented Anyue ceramic-pot sealed meat mainly include ethanol, acetaldehyde, 1-octene-3-alcohol, 3-hydroxy-2-butanone, acetic acid and ethyl acetate. Moreover, the characteristic flavor substances in Anyue ceramic-pot sealed meat produced in different seasons were different. Isoamyl alcohol, 2,2,4,6,6-pentamethylheptane, 4-hydroxy-2-butanone and ethyl propionate may be the characteristic flavor substances of Anyue ceramic-pot sealed meat produced in January. Amyl formate, furan, acetone, n-hexane and carbon disulfide may be the characteristic flavor substances of Anyue ceramic-pot sealed meat produced in April. 1,3,5-trimethylbenzene may be the characteristic flavor substance of Anyue ceramic-pot sealed meat produced inJuly. Butyl acetate, ethyl propionate, 3-ethyl-2,5-methylpyrazine, 1,3-divinylbenzene and n-ethylpropionamide may be the characteristic flavor substance of Anyue ceramic-pot sealed meat produced in October. Low temperature and long term fermentation was beneficial to the formation of characteristic flavor substances in Anyue ceramic-pot sealed meat.

Publication Date

2-18-2023

First Page

12

Last Page

17,104

DOI

10.13652/j.issn.1003-5788.2020.12.003

References

[1] 侯婷婷,刘鑫,田学宗,等.火腿风味的低钠发酵肉制品品质及风味研究[J].食品与机械,2019,35(12):185-189.
[2] 廖定容.罐罐肉加工与贮藏过程中风味形成机理的初步研究[D].雅安:四川农业大学,2013:2-7.
[3] 汪修意,徐文泱,陈同强,等.气相色谱—质谱联用与相对气味活度值法分析坛子肉风味物质的研究[J].食品安全质量检测学报,2019,10(24):8 450-8 455.
[4] BOLZONI L,BARBIER G,VIRGILI R.Changes in volatile compounds of Parma Ham during maturation[J].Meat Science,1996,43:301-310.
[5] 田怀香,王璋.热脱附—气质联用分析金华火腿挥发性风味[J].食品与机械,2007,23(3):10-12,69.
[6] 李佳,刘忠义,付满,等.发酵香肠风味物质气质分析及与发酵时间的关系[J].食品与机械,2019,35(5):61-66.
[7] 陆应林.南京板鸭加工过程中蛋白降解及风味物质的研究[D].南京:南京农业大学,2012:5-12.
[8] 周才琼,代小容,杜木英.酸肉发酵过程中挥发性风味物质形成的研究[J].食品科学,2010,31(7):98-104.
[9] 陈竞适,刘静,任海姣,等.湘西陈年腊肉微生物群落分析及高产脂肪酶细菌的筛选[J].肉类研究,2017,31(3):1-6.
[10] 刘有晴,黄丹,于华,等.四川腊肉中乳酸菌的筛选、产酸特性及其氨基酸产物分析[J].食品与机械,2016,32(1):34-37.
[11] 易宇文,刘阳,彭毅秦,等.东坡肘子风味电子鼻分析与感官评定相关性探究[J].食品与发酵工业,2018,44(1):238-244.
[12] 范文教,易宇文,徐培,等.电子舌技术识别掺假腐肉香肠的研究[J].食品工业,2017,38(12):159-163.
[13] XAVIER C,ANDREU G C,NORA C,et al.Electronic tongues to assess wine sensory descriptors[J].Talanta,2017,162:218-224.
[14] ZHOU Hua-ying,LUO De-han,GHOLAM H H,et al.Identification of Chinese herbal medicines with electronic nose technology:Applications and challenges[J].Sensors,2017,17(5):1 073.
[15] 叶芳艳,左木林,朱万龙,等.HS-SPME-GC/MS法分析中缅树鼩尿液的化学成分[J].兽类学报,2018,38(1):85-94.
[16] MOTILVA M J,TOLDRA F,NIETO P,et al.Muscleli-polysis phenomenain the processing of dry-curedham[J].Food Chemistry,1993,48(2):121-125.
[17] PAN B S,KOU J M.Flavor of shell fish and Kamabokoil-avourants[M].New York:Blaekie Aeadmicand Professional,1994:85-114.
[18] BERDAGUE J L,DENOYER C,LE QUERE J L,et al.Volatile components of dry-cured ham[J].Journal of Agricultural and Food Chemistry,1991,39(7):1 257-1 261.
[19] 乔发东,马长伟.宣威火腿加工过程中挥发性风味化合物分析[J].食品研究与开发,2006,27(3):24-29.
[20] 张发庆.有机化学[M].北京:化学工业出版社,2012:200-204.
[21] FLORES M,SPANIER A M,TOLDRA F.Flavor analysis of dry-cured ham[M].[S.l.]:Aspen Publishers Inc,1998:320-341.

Share

COinS
 
 

To view the content in your browser, please download Adobe Reader or, alternately,
you may Download the file to your hard drive.

NOTE: The latest versions of Adobe Reader do not support viewing PDF files within Firefox on Mac OS and if you are using a modern (Intel) Mac, there is no official plugin for viewing PDF files within the browser window.