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Abstract

Objective:In order to optimize the process parameters of tobacco sheet of heated cigarette. Methods:12 gradient grades of tobacco sheets with glycerol addition ratio of 5%~30% were prepared under laboratory conditions. The mass of moisture, nicotine and glycerol in heated cigarette smoke, filter condensation section and tobacco core section were detected by GC-TCD method. And the mass distribution characteristics of main components, release rate, filtration rate and transfer rate were analyzed. Results:When 5%~30% glycerol was applied to the heated cigarette tobacco sheets, the water release rate was 88.6%~92.3%, which was mainly distributed in the smoke and filter condensation section; The nicotine release rate was 25.5%~34.2%, which was mainly distributed in the filter condensing section and tobacco core section; The glycerol release rate was 13.9%~21.3%, which was mainly distributed in the tobacco core section. Conclusion:When 10%~18% glycerol was added to tobacco sheets, nicotine and glycerol in heated cigarettes had higher transfer rate and lower filtration rate.

Publication Date

11-23-2022

First Page

43

Last Page

49

DOI

10.13652/j.spjx.1003.5788.2022.90120

References

[1] 刘珊,崔凯,曾世通,等.加热非燃烧型烟草制品剖析[J].烟草科技,2016,49(11):56-65.LIU S,CUI K,ZENG S T,et al.Analysis of blend and aerosol composition of two heatnotburn tobacco products[J].Tobacco Science & Technology,2016,49(11):56-65.
[2] 刘亚丽,王金棒,郑新章,等.加热不燃烧烟草制品发展现状及展望[J].中国烟草学报,2018,24(4):91-106.LIU Y L,WANG J B,ZHENG X Z,et al.Current status and prospect of heat-not-burn tobacco products[J].Acta Tabacaria Sinica,2018,24(4):91-106.
[3] 窦玉青,沈轶,杨举田,等.新型烟草制品发展现状及展望[J].中国烟草科学,2016,37(5):92-97.DOU Y Q,SHEN Y,YANG J T,et al.The development and prospect of novel tobacco products[J].Chinese Tobacco Science,2016,37(5):92-97.
[4] BORGERDING M F,BODNAR J A,CHUNGH L,et al.Chemical and biological studies of a new cigarette that primarily heats tobacco Part 1:Chemical composition of mainstream smoke[J].Food & Chemical Toxicology,1998,36(3):169-182.
[5] 周昆,杨继,杨柳,等.加热不燃烧卷烟烟气气溶胶研究进展[J].中国烟草学报,2017,23(5):141-149.ZHOU K,YANG J,YANG L,et al.Research advances related to heat not burn tobacco aerosol[J].Acta Tabacaria Sinica,2017,23(5):141-149.
[6] 刘鸿,陶立奇,陆怡峰,等.加热烟草制品(HTPs)气溶胶成分的MD-GC/MS分析[J].中国烟草学报,2020,26(3):9-14.LIU H,TAO L Q,LU Y F,et al.Composition analysis of heated tobacco products(HTPs)aerosol by MD-GC/MS[J].Acta Tabacaria Sinica,2020,26(3):9-14.
[7] BAKERR R.Smoke generation inside a burning cigarette:Modifying combustion to develop cigarettes that may be less hazardous to health[J].Energy & Combustion Science,2006,32(4):373-385.
[8] BOMBICK B R,MURLI H,AVALOS J T,et al.Chemical and biological studies of a new cigarette that primarily heats tobacco Part 2:In vitro toxicology of mainstream smoke condensate[J].Food & Chemical Toxicology,1998,36(3):183-190.
[9] KOGEL U,SCHLAGE W K,MARTIN F,et al.A 28-day rat inhalation study with an integrated molecular toxicology endpoint demonstrates reduced exposure effects for a prototypic modified risk tobacco product compared with conventional cigarettes[J].Food & Chemical Toxicology,2014,68(1):204-217.
[10] 李翔,谢复炜,刘惠民.新型烟草制品毒理学评价研究进展[J].烟草科技,2016(1):88-93.LI X,XIE F W,LIU H M.Recent advances in toxicological evaluation of novel tobacco products[J].Tobacco Science & Technology,2016(1):88-93.
[11] 董高峰,田永峰,尚善斋,等.用于加热不燃烧(HnB)卷烟的再造烟叶生产工艺研究进展[J].中国烟草学报,2020,26(1):109-117.DONG G F,TIAN Y F,SHANG S Z,et al.Production technology of reconstituted tobacco for heat-not-burn(HnB)cigarettes:A review[J].Acta Tabacaria Sinica,Acta Tabacaria Sinica,2020,26(1):109-117.
[12] 张园园,唐婷婷,张佳琳,等.加热不燃烧烟草薄片发展现状及其展望[J].中华纸业,2020,41(18):14-17.ZHANG Y Y,TANG T T,ZHANG J L,et al.Development status and prospect on heating non-combustible reconstituted tobacco[J].China Pulp & Paper Industry,2020,41(18):14-17.
[13] 张金廷,胡培强,施永诚,等.甘油[M].北京:化学工业出版社,2008:109-112.ZHANG J T,HU P Q,SHI Y C,et al.Glycerol[M].Beijing:Chemical Industry Press,2008:109-112.
[14] 孙平,张津凤,姚秀玲.化工产品手册:食品添加剂[M].北京:化学工业出版社,2016:96-97.SUN P,ZHANG J F YAO X L.Chemical products manual:Food additives[M].Beijing:Chemical Industry Press,2016:96-97.
[15] 周慧明,刘鸿,刘广超,等.自制研究平台不同加热温度下电加热卷烟主要成分的释放行为[J].烟草科技,2021,54(6):50-57.ZHOU H M,LIU H,LIU G C,et al.Release behaviors of main aerosol components from electrically heated cigarettes at different temperatures based on a bespoke test platform[J].Tobacco Science & Technology,2021,54(6):50-57.
[16] 龚淑果,刘魏,黄平,等.加热不燃烧卷烟烟气主要成分的逐口释放行为[J].烟草科技,2019,52(2):62-71.GONG S G,LIU W,HUANG P,et al.Puff-by-puff release of main aerosol components from two commercial heat-not-burn tobacco products[J].Tobacco Science & Technology,2019,52(2):62-71.
[17] 张洪非,姜兴益,庞永强,等.两种抽吸模式下加热不燃烧卷烟主流烟气释放物分析[J].烟草科技,2018,51(9):40-48.ZHANG H F,JIANG X Y,PANG Y Q,et al.Analysis of mainstream aerosol emissions of heat-not-burn tobacco products under two puffing regimes[J].Tobacco Science & Technology,2018,51(9):40-48.
[18] 赵光飞,刘静,屠彦刚,等.气相色谱法同时检测加热不燃烧卷烟芯材中的1,2-丙二醇、烟碱与甘油含量[J].中国测试,2019,45(3):69-74.ZHAO G F,LIU J,TU Y G,et al.Simultaneous determination of 1,2-propylene glycol,nicotine and glycerol in heat-not-burn cigarette core material by gas chromatography method[J].China Measurement & Testing Technology,2019,45(3):69-74.
[19] 王康,柳均,肖少红,等.GC-TCD法同时检测加热不燃烧卷烟烟气气溶胶水分,及烟碱、丙三醇、1,2-丙二醇、三乙酸甘油酯和薄荷醇的释放量[J].烟草科技,2019,52(3):63-68.WANG K,LIU J,XIAO S H,et al.Simultaneous determination of moisture content and deliveries of nicotine,glycerol,1,2-propylene glycol,glycerol triacetate and menthol in aerosol from heat-not-burn tobacco products by GC-TCD method[J].Tobacco Science & Technology,2019,52(3):63-68.
[20] 肯生叶,温光和,杨雪燕,等.GC-TCD法同时检测加热不燃烧卷烟烟草材料中的水分、1,2-丙二醇、烟碱和丙三醇[J].烟草科技,2020,53(5):46-55.KEN S Y,WEN G H,YANG X Y,et al.Simultaneous determination of moisture,1,2-propylene glycol,nicotine and glycerol in tobacco material for heat-not-burn products by GC-TCD[J].Tobacco Science & Technology,2020,53(5):46-55.
[21] 张丽,王维维,张小涛,等.加热不燃烧卷烟气溶胶中主要成分的转移行为[J].烟草科技,2019,52(3):46-55.ZHANG L,WANG W W,ZHANG X T,et al.Transfer behavior of main aerosol components in heat-not-burn tobacco products[J].Tobacco Science & Technology,2019,52(3):46-55.
[22] 刘鸿,张怡春,陆怡峰,等.电子烟气溶胶成分释放的主要影响因素[J].烟草科技,2020,53(10):39-45.LIU H,ZHANG Y C,LU Y F,et al.Main factors affecting aerosol component releases from e-cigarette[J].Tobacco Science & Technology,2020,53(10):39-45.
[23] 杨雪燕,温光和,李峰,等.加热不燃烧卷烟烟草材料的特性分析[J].食品与机械,2020,36(5):205-210.YANG X Y,WEN G H,LI F,et al.Characteristic analysis of heat-not-burn cigarette tobacco materials[J].Food & Machinery,2020,36(5):205-210.
[24] 唐培培,曾世通,刘珊,等.甘油对烟叶热性能及加热状态下烟气释放的影响[J].烟草科技,2015,48(3):61-65.TANG P P,ZENG S T,LIU S,et al.Effects of glycerol on thermal property and smoke release of tobacco leaves under heating[J].Tobacco Science & Technology,2015,48(3):61-65.
[25] 赵龙,刘珊,曾世通,等.甘油对烟丝加热状态下烟气中挥发性和半挥发性成分的影响[J].烟草科技,2016,49(4):53-60.ZHAO L,LIU S,ZENG S T,et al.Influence of glycerol on release of volatile and semi-volatile chemical components in cut tobacco under heating[J].Tobacco Science & Technology,2016,49(4):53-60.
[26] 周慧明,华青,刘广超,等.加热非燃烧状态下烟草制品的TSNAs释放规律[J].中国烟草科学,2019,40(1):82-88.ZHOU H M,HUA Q,LIU G C,et al.TSNAs release of heat-not-burn tobacco materials[J].Chinese Tobacco Science,2019,40(1):82-88.
[27] 黄嘉礽.卷烟工艺[M].北京:北京出版社,2000:401-406.HUANG J R.Cigarette technology[M].Beijing:Beijing Press,2000:401-406.

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