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Corresponding Author(s)

张哲(1975—),男,天津商业大学教授,博士。E-mail: zhang zhe @tjcu.edu.cn

Abstract

Objective: This study aimed to obtain optimal sublimation temperature of pear melon cells. Methods: The pre-freezing cooling rate and vacuum pressure were selected by optimization method to be 25 ℃/min and 10 Pa, respectively, based on cryogenic microscope imaging and vacuum freeze-drying technology. Then, sublimation temperatures of 10, 5, 0, -4, -7 and -10 ℃ were used for experimental research. The morphological parameters (equivalent diameter, area, circumference, volume), internal pressure, and porosity of cells during the process of dehydration and drying were analyzed. Results: As the sublimation temperature rose, the morphological parameters of different dimensions of cells first decreased and subsequently increased. The change rates of equivalent diameter, cross-sectional area, and volume of cells were 5.05%, 9.60%, and 14.68% after drying at 0 ℃, which well preserved the original morphological structure of cells. At the same time, with the increase of dimension, the change amount at the same sublimation temperature also increases. Conclusion: Combined with the optimal pre-freezing rate and vacuum degree, the optimum temperature condition of pear melon drying sublimation is 0 ℃.

Publication Date

12-26-2023

First Page

12

Last Page

17,44

DOI

10.13652/j.spjx.1003.5788.2023.80313

References

[1] 李兢思, 李俊欣, 付佳佳. 冷冻干燥技术及其在食品加工行业的应用[J]. 食品安全导刊, 2022(34): 151-158. LI J S, LI J X, FU J J. Freeze drying technology and its application in food processing industry[J]. Food Safety Guide, 2022(34): 151-158.
[2] KROKIDA M K, KARATHANOS V T, MAROULIS Z B. Effect of freeze-drying conditions on shrinkage and porosity of dehydrated agricultural products[J]. Journal of Food Engineering, 1998, 35(4): 53-56.
[3] 毕金峰, 冯舒涵, 金鑫, 等. 真空冷冻干燥技术与产业的发展及趋势[J]. 核农学报, 2022, 36(2): 414-421. BI J F, FENG S H, JIN X, et al. Development and trend of vacuum freeze drying technology and industry[J]. Journal of Nuclear Agricultural Science, 2022, 36(2): 414-421.
[4] WAGHMARE R, KUMAR M, YADAV R, et al. Application of ultrasonication as pre-treatmeat for freeze drying: An innovation approach for the retention of nutraceutical quality in food[J]. Food Chemistry, 2023, 404: 79-86.
[5] 蔡路昀, 台瑞瑞, 曹爱玲, 等. 冷冻因素对水产品品质的影响及冷冻保鲜的研究进展[J]. 食品工业科技, 2018, 39(20): 308-319. CAI L Y, TAI R R, CAO A L, et al. Effect of freezing factors on the quality of aquatic products and the research progress in freezing preservation[J]. Science and Technology of Food Industry, 2018, 39(20): 308-319.
[6] 王元春, 谢晓航, 黄忠闯, 等. 芒果冷冻干燥过程中营养成分变化的研究[J]. 食品工业, 2011, 32(12): 65-68. WANG Y C, XIE X H, HUANG Z C, et al. Study on the change of nutrient composition of mango during freeze drying[J]. Food Industry, 2011, 32(12): 65-68.
[7] SAPKOTA G, DELGADO E, VANLEEUWEN D, et al. Preservation of phenols, antioxidant activity, and cyclic adenosine monophosphate in jujube (Ziziphus jujuba mill.) fruits with different drying methods[J]. Plants, 2023, 12(9): 98-104.
[8] FISSORE D, GALLO G, RUGGIERO A E, et al. On the use of a micro freeze-dryer for the investigation of the primary drying stage of a freeze-drying process[J]. European Journal of Pharmaceutics and Biopharmaceutics, 2019, 141: 121-129.
[9] 诸凯, 董杨, 王雅博, 等. 脱水过程对细胞骨架的影响[J]. 制冷学报, 2020, 41(4): 159-166. ZHU K, DONG Y, WANG Y B, et al. Effect of dehydration on cytoskeleton[J]. Journal of Refrigeration, 2020, 41(4): 159-166.
[10] 徐海龙, 于莹, 赵明波. 响应面法优化黑果腺肋花楸真空冷冻干燥工艺[J]. 现代农业科技, 2022(22): 189-193. XU H L, YU Y, ZHAO M B. Optimization of vacuum freeze-drying process of sorbus melanocarpa by response surface method[J]. Modern Agricultural Science and Technology, 2022(22): 189-193.
[11] 袁小峰, 阮征, 张飞, 等. 正交试验优化蜜柚真空冷冻干燥工艺[J]. 食品研究与开发, 2022, 43(18): 100-105. YUAN X F, RUAN Z, ZHANG F, et al. Optimization of vacuum freeze drying process of honey pomelo by orthogonal experiment[J]. Food Research and Development, 2022, 43(18): 100-105.
[12] 张艳红. 胡萝卜真空冷冻干燥试验[J]. 农业工程, 2019, 9(11): 52-55. ZHANG Y H. Experiment on vacuum freeze drying of carrot[J]. Agricultural Engineering, 2019, 9(11): 52-55.
[13] 王泽智. 基于干燥特性及品质控制的葱茎段预处理联合真空冷冻干燥研究[D]. 镇江: 江苏大学, 2022: 9. WANG Z Z. Study on pretreatment of onion stem segment combined with vacuum freeze-drying based on drying characteristics and quality control[D]. Zhenjiang: Jiangsu University, 2022: 9.
[14] 罗洁莹, 汤梅, 柳建良, 等. 蓝莓真空冷冻干燥工艺优化[J]. 食品研究与开发, 2018, 39(3): 91-95. LUO J Y, TANG M, LIU J L, et al. Optimization of vacuum freeze-drying process for blueberry[J]. Food Research and Development, 2018, 39(3): 91-95.
[15] 魏丽红, 翟秋喜. 软枣猕猴桃真空冷冻干燥条件的筛选[J]. 辽宁农业职业技术学院学报, 2019, 21(5): 7-9. WEI L H, ZHAI Q X. Screening of vacuum freeze-drying conditions for actinidia jujube[J]. Journal of Liaoning Agricultural Vocational and Technical College, 2019, 21(5): 7-9.
[16] 郭利琴. 蒜片真空冷冻干燥工艺及其贮藏包装的研究[D]. 太原: 山西农业大学, 2020: 23. GUO L Q. Research on vacuum freeze drying technology and storage packaging of garlic slices[D]. Taiyuan: Shanxi Agricultural University, 2020: 23.
[17] 徐垚. 贮运过程中果蔬细胞组织损伤机理微观实验研究[D]. 天津: 天津商业大学, 2019: 28. XU Y. Microscopic experimental study on damage mechanism of fruit and vegetable cell tissue during storage and transportation[D]. Tianjin: Tianjin University of Commerce, 2019: 28.
[18] 柯程虎, 张辉, 保秀娟. 团聚形核壳结构冰晶粒子的激光散射特性[J]. 红外与激光工程, 2019, 48(8): 70-76. KE C H, ZHANG H, BAO X J. Laser emission characteristics of agglomerated core-shell ice crystal particles[J]. Infrared and Laser Engineering, 2019, 48(8): 70-76.
[19] 张彤. 火龙果真空冷冻干燥热质传递理论与实验研究[D]. 上海: 上海海洋大学, 2022: 4. ZHANG T. Theoretical and experimental study on heat and mass transfer in vacuum freeze drying of pitaya fruit[D]. Shanghai: Shanghai Ocean University, 2022: 4.
[20] 张爱琳. 香蕉预冻过程传热性能及真空冷冻干燥工艺优化研究[D]. 哈尔滨: 哈尔滨商业大学, 2020: 44. ZHANG A L. Study on heat transfer performance and vacuum freeze-drying process optimization of bananas during pre-freezing[D]. Harbin: Harbin University of Commerce, 2020: 44.
[21] 易丽, 杨薇, 王晨, 等. 番木瓜片真空冷冻干燥工艺研究[J]. 农产品加工, 2016(17): 19-22. YI L, YANG W, WANG C, et al. Study on vacuum freeze-drying technology of papaya slices[J]. Processing of Agricultural Products, 2016(17): 19-22.
[22] 高续春, 代宏哲, 樊君, 等. 红枣冻干升华工艺优化研究[J]. 当代化工, 2009, 38(4): 335-339. GAO X C, DAI H Z, FAN J, et al. Optimization of freeze-drying and sublimation process for red jujube[J]. Contemporary Chemical Industry, 2009, 38(4): 335-339.
[23] 郭帅帅. 冷冻干燥中传热传质过程的实验和数值模拟研究[D]. 青岛: 青岛大学, 2021: 46. GUO S S. Experimental and numerical simulation of heat and mass transfer in freeze-drying[D]. Qingdao: Qingdao University, 2021: 46.
[24] 王雅博, 诸凯, 代宝民, 等. 冷却速率对洋葱内表皮细胞结构的影响[J]. 制冷学报, 2018, 39(6): 129-134. WANG Y B, ZHU K, DAI B M, et al. Effect of cooling rate on cell structure of inner epidermis of onion[J]. Journal of Refrigeration, 2018, 39(6): 129-134.
[25] 赵延强. 具有初始孔隙多孔物料冷冻干燥的实验研究[D]. 大连: 大连理工大学, 2015: 27. ZHAO Y Q. Experimental study on freeze drying of porous materials with initial porosity from aqueous solution[D]. Dalian: Dalian University of Technology, 2015: 27.

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