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Corresponding Author(s)

李嘉欣(1989—),女,贵州中医药大学药学院讲师,博士。E-mail:carry556@126.com

Abstract

[Objective] To establish a fast,sensitive,and accurate method for detecting carmine.[Methods] Using Folium Nelumbinis;as the carbon source,carbon dots (FN-CDs ) were prepared using a solvent thermal method,and the preparation conditions were optimized using a single factor test.Study the factors that affect the fluorescence intensity of FN -CDs,the effects of coexisting substances on the detection system,and optimize the measurement conditions;Using FN -CDs for the determination of carmine content in food and exploring its mechanism of action.[Results]] Using 0.6 g of Folium Nelumbinis,0.25 g of citric acid and 45 mL of formamide were reacted at 240 ℃ for 4 hours,and the fluorescence value of FN -CDs was the strongest.Rouge had a good linear relationship within the concentration range of 0~70 µg/mL,with an R2 of 0.996 4 and a detection limit of 0.57 µg/mL.The spiked recovery rates of grapefruit juice beverage and canned arbutu were 88.09%~102.49% and 97.73%~112.47%,respectively.[Conclusion] This detection method has the characteristics of high sensitivity,good selectivity and high accuracy,and can be applied to the rapid detection of carmine in food.

Publication Date

2-18-2025

First Page

54

Last Page

60

DOI

10.13652/j.spjx.1003.5788.2024.80411

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