Abstract
［Objective］ To establish a rapid detecting method for the determination of dimethyl fumarate in beverages by ultrasound -assisted dispersive liquid -liquid micro -extraction coupled with high performance liquid chromatography.［Methods］ The beverage samples were spiked with extractant and dispersant,extracted by ultrasonic extraction,centrifuged and determined by high performance liquid chromatography.［Results］ The optimal microextraction conditions were 100 μL of chloroform as extractant,300 μL of acetone as dispersant,and a sonication time of 4 min.Under the optimal extraction conditions,dimethyl fumarate had a linear range of 0.1~100.0 μg/mL with a detection limit of 0.02 μg/L.The relative standard deviation (RSD ) of the method was less than 3.7%,and the spike recovery rate was between 75.0% and 85.0%.［Conclusion］ The method is simple,rapid,reproducible,sensitive and environmentally friendly,and is suitable for the qualitative and quantitative analysis of dimethyl fumarate in beverages.
Publication Date
4-3-2025
First Page
80
Last Page
85
DOI
10.13652/j.spjx.1003.5788.2023.81272
Recommended Citation
Fangjun, JIANG; Feng, LIANG; Yalong, FENG; Qiuyi, LI; Fanglin, DING; and Zhaohui, ZHANG
(2025)
"Rapid determination of dimethyl fumarate in beverages by dispersed liquid-liquid microextraction with ultrasound-assisted and high performance liquid chromatography,"
Food and Machinery: Vol. 41:
Iss.
1, Article 10.
DOI: 10.13652/j.spjx.1003.5788.2023.81272
Available at:
https://www.ifoodmm.cn/journal/vol41/iss1/10
References
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