Abstract
[Objective] To improve the accuracy and reliability of the titration method for determining the peroxide value in rapeseed oil.[Methods] The peroxide value in rapeseed oil is determined using the titration method,and a mathematical model is established to analyze the sources of uncertainty.The uncertainty components are evaluated,and the combined uncertainty is calculated.[Results]] When the peroxide value in rapeseed oil is 0.043 g/100 g,the expanded uncertainty is ±0.001 06 g/100 g (k=2).[Conclusion] The factors that mainly influence the uncertainty of the measurement results are the repeatability of sample measurement and titration volume.Other factors have a relatively smaller effect.Using high -precision Class A burettes and increasing the number of parallel measurements can reduce the uncertainty of the detection.
Publication Date
7-11-2025
First Page
51
Last Page
55
DOI
10.13652/j.spjx.1003.5788.2024.80881
Recommended Citation
Ru, WANG; Lijuan, CHANG; Yang, CHEN; and Mingjin, ZHANG
(2025)
"Determination of uncertainty in peroxide value of rapeseed oil by titration method,"
Food and Machinery: Vol. 41:
Iss.
7, Article 8.
DOI: 10.13652/j.spjx.1003.5788.2024.80881
Available at:
https://www.ifoodmm.cn/journal/vol41/iss7/8
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