Abstract
[Objective] To explore the preferred conditions for thermal sterilization of Korean rice wine from the perspective of aroma component preservation. [Methods] The effects of different thermal sterilization conditions on the aroma quality of traditional Korean rice wine are evaluated by combining an electronic nose with headspace solid-phase microextraction gas chromatography-mass spectrometry (HS-SPME-GC-MS). The response values of the electronic nose sensors, as well as the types and content of volatile compounds, are determined. [Results] The response signals of the sensors R7 (inorganic sulfides), R9 (organic sulfides), R2 (nitrogen oxides), R6 (methyls), and R8 (alcohols and aldehydes and ketones) to different heat sterilized samples are generally strong. Linear discriminant analysis (LDA) shows that the volatile compounds of the rice wine samples sterilized at 65 ℃ for 5 min are the most similar to those of the unpasteurized samples. In contrast, the original flavor profiles of the samples are significantly altered by sterilizing the samples at 85 ℃ for 30 min and 125 ℃ for 5 s. A total of 106 aroma compounds are identified in the four groups of rice wine samples, with alcohols and esters being the most abundant. Their relative content is 25.53%~40.67% and 33.49%~44.75%, respectively. Thermal sterilization affects both the types and relative content of volatile compounds in the samples. The rice wine sterilized at 65 ℃ for 5 min exhibits the closest similarity to unsterilized rice wine, with total mass concentrations of compounds being 7.26 and 8.74 mg/L, respectively. [Conclusion] Based on aroma component analysis, sterilization at 65 ℃ for 5 min is identified as the preferred thermal sterilization condition for traditional Korean rice wine.
Publication Date
5-13-2026
First Page
167
Last Page
175
DOI
10.13652/j.spjx.1003.5788.2025.80547
Recommended Citation
Weiliang, XIA; Tieyan, JIN; and Sirui, XIONG
(2026)
"Effects of thermal sterilization conditions on the aromatic quality of traditional Korean rice wine,"
Food and Machinery: Vol. 42:
Iss.
3, Article 21.
DOI: 10.13652/j.spjx.1003.5788.2025.80547
Available at:
https://www.ifoodmm.cn/journal/vol42/iss3/21
References
[1] HE Y,WANG X Y,LI P H,et al.Research progress of wine aroma components:a critical review [J].Food Chemistry,2023,402:134491.
[2] HUANG M Z,LIU X Z,LI X,et al.Effect of Hanseniaspora uvarum - Saccharomyces cerevisiae mixed fermentation on aroma characteristics of Rosa roxburghii tratt,blueberry,and plum wines [J].Molecules,2022,27(22):8 097.
[3] CHIOZZI V,AGRIOPOULOU S,VARZAKAS T.Advances,applications,and comparison of thermal (pasteurization,sterilization,and aseptic packaging) against non-thermal (ultrasounds,UV radiation,ozonation,high hydrostatic pressure) technologies in food processing [J].Applied Sciences,2022,12(4):2 202.
[4] BAO S H,YIN D Z,ZHAO Q Y,et al.Comprehensiveevaluation of the effect of five sterilization methods on the quality of black carrot juice based on PCA,TOPSIS and GRA models [J].Food Chemistry:X,2023,17:100604.
[5] 孙方丹,金铁岩.2种杀菌处理对朝鲜族米酒品质影响的研究[J].延边大学农学学报,2019,41(1):73-78,86.SUN F D,JIN T Y.Research on the effect of two sterilization treatment methods on the quality of Korean rice wine [J].Agricultural Science Journal of Yanbian University,2019,41(1):73-78,86.
[6] 张 玲.朝 鲜 族 米 酒 最 适 杀 菌 方 法 研 究 [D].延 吉:延 边 大 学,2016:13-15.ZHANG L.Study on optimum sterilization method of Korean ethnic rice wine [D].Yanji:Yanbian University,2016:13-15.
[7] 熊思瑞,王龙宇,王云峰,等.超高温瞬时灭菌对米酒品质的影响 [J].食品与机械,2024,40(1):183-188,218.XIONG S R,WANG L Y,WANG Y F,et al.Effect of ultra-high temperature transient sterilization on quality of rice wine [J].Food & Machinery,2024,40(1):183-188,218.
[8] 闫海峡,杨钧翔,刘彦君,等.乳脂肪含量对超高温瞬时灭菌乳感官品质的影响 [J].沈阳农业大学学报,2023,54(6):741-747.YAN H Y,YANG J X,LIU Y J,et al.Effects of milk fat content on the sensory quality of ultra-high temperature milk [J].Journal of Shenyang Agricultural University,2023,54(6):741-747.
[9] POLAK N,KALISZ S,KRUSZEWSKI B.High-temperature short-time and ultra-high-temperature processing of juices,nectars and beverages:influences on enzyme,microbial inactivation and retention of bioactive compounds [J].Applied Sciences,2024,14(19):8 978.
[10] 吴吉玲,黄一珍,姜鹏飞,等.排序法在大西洋鲭鱼脱腥工艺筛选中的应用 [J].食品研究与开发,2020,41(23):73-79.WU J L,HUANG Y Z,JIANG P F,et al.Application of ranking test in screening of Atlantic mackerel (Scomber scombrus) deodorization process [J].Food Research and Development,2020,41(23):73-79.
[11] FANG D L,YANG W J,KIMATU B M,et al.Comparison of flavour qualities of mushrooms (Flammulina velutipes) packed with different packaging materials [J].Food Chemistry,2017,232:1-9.
[12] 刘浩,赵生满,任贵兴.顶空固相微萃取结合气质联用分析小米黄酒与黍米黄酒的香气成分 [J].酿酒科技,2015 (1):115-119,123.LIU H,ZHAO S M,REN G X.Analysis of flavoring components of yellow rice wine made by millet or husked millet by head-space solid phase micro-extraction coupled with gas chromatography-mass spectrometry [J].Liquor-Making Science & Technology,2015 (1):115-119,123.
[13] 彭旭怡,郑经绍,刘宇航,等.基于电子鼻、顶空气相色谱—离子迁移谱分析比较不同杀菌处理紫米甜酒酿中的挥发性成分 [J].现代食品科技,2021,37(7):259-268.PENG X Y,ZHENG J S,LIU Y H,et al.Analysis and comparison of volatile components in purple rice sweet wine with different sterilization treatments by electronic nose and headspace gas chromatography-ion mobility spectrometry [J].Modern Food Science and Technology,2021,37(7):259-268.
[14] 管照奕珠,方芳,王耀耀,等.电子鼻技术结合化学计量学快速鉴别掺假茶籽油 [J].食品与机械,2023,39(6):31-36,179.GUAN Z Y Z,FANG F,WANG Y Y,et al.Rapid identification of adulterated camellia seed oil by e-nose combined with chemometrics [J].Food & Machinery,2023,39(6):31-36,179.
[15] 吴林,袁雪,马靖童,等.猕猴桃苹果复合果酒低温发酵工艺优化及品质分析 [J].中国酿造,2023,42(12):153-160.WU L,YUAN X,MA J T,et al.Optimization of low-temperature fermentation technology and quality analysis of kiwi-apple compound fruit wine [J].China Brewing,2023,42(12):153-160.
[16] 姬中伟,衡洋洋,周志磊,等.超高温瞬时杀菌对苏派黄酒风味物质的影响 [J].食品与发酵工业,2022,48(10):16-21.JI Z W,HENG Y Y,ZHOU Z L,et al.Effect of ultra-high temperature instantaneous sterilization on flavor substances in Supai Huangjiu [J].Food and Fermentation Industries,2022,48(10):16-21.
[17] 黄小兰,何旭峰,熊双,等.外碳源对猕猴桃酒品质及挥发性成分的影响 [J].食品与机械,2024,40(10):39-45.HUANG X L,HE X F,X S,et al.Effects of external carbon sources on the quality and volatile components of kiwi wine[J].Food & Machinery,2024,40(10):39-45.
[18] 苏佳佳.糙米酒酿制备工艺及其品质特性研究 [D].无锡:江南大学,2020:23-28.SU J J.Study on preparation technology and quality characteristics of brown rice wine [D].Wuxi:Jiangnan University,2020:23-28.
[19] TUFARIELLO M,CAPONE S,SICILIANO P.Volatile components of Negroamaro red wines produced in Apulian Salento area [J].Food Chemistry,2012,132(4):2 155-2 164.
[20] 吴琼,冯卫敏,蒋和体.不同杀菌方式对桑葚原汁品质的影响[J].食品科学,2016,37(9):144-149.WU Q,FENG W M,JIANG H T.Effect of sterilization methods on the quality of mulberry juice [J].Food Science,2016,37(9):144-149.
[21] 何洋,冯怡婷,吴昊文,等.云南米酒中优质酵母协同米根霉发酵对米酒理化性质及风味物质的影响 [J].食品工业科技,2025,46(12):173-183.HE Y,FENG Y T,WU H W,et al.Effects of synergistic fermentation of yeast in Yunnan rice wine and rhizopus oryzae on physicochemical properties and flavor substances of rice wine [J].Science and Technology of Food Industry,2025,46(12):173-183.
[22] 屠婷瑶,向玲,王红梅,等.不同地区发酵型米酒挥发性风味化合物研究 [J].食品安全质量检测学报,2024,15(20):176-185.TU T Y,XIANG L,WANG H M,et al.Study on volatile flavor compounds of fermented rice wine in different regions [J].Journal of Food Safety & Quality,2024,15(20):176-185.
